Makowiec, Mary E., and Thierry A. Blanchet. Wear, 2017, 374, 77-85.
Microfillers have been shown to significantly reduce the wear rate of PTFE, such as α-alumina and activated nanocarbon. This work explored the wear reduction properties of more carbon-based nanomaterials on PTFE, including functionalized and non-functionalized multi-walled carbon nanotubes and mesoporous nanocarbon. The results showed that carboxyl functionalized carbon nanotubes and mesoporous nanocarbons were both effective nanoscale fillers compared to non-functionalized multi-walled carbon nanotubes, and the wear rate of the composites was close to 10-7 mm3/Nm.
Preparation of PTFE composites filled with carbon nanomaterials
· The preparation process of carbon nanomaterial-filled PTFE composites involves blending PTFE powder with various carbon fillers, including carbon nanotubes, mesoporous nanocarbon, and micrographite.
· The composite powders are mixed by hand and then with a Hauschild mixer, pressed into pucks, and sintered in a nitrogen environment at 360 °C for 3 hours.
· The sintered pucks are then cut into pins for testing in a reciprocating pin-on-flat tribometer. The pins undergo sliding against stainless steel countersurfaces at room temperature, with wear rates measured at various intervals. Steady-state wear rates are determined from the wear record, with a 95% confidence interval obtained for each data point.